亚临界流体萃取马鲛鱼加工下脚料中鱼油的研究
PDF下载 (870)毛丽芳,朱新亮,桑卫国.亚临界流体萃取马鲛鱼加工下脚料中鱼油的研究[J].宁波大学学报(理工版),2012,25(04):10-15.DOI:
MAO Li-fang,ZHU Xin-liang,SANG Wei-guo.Fish Oil Extraction from By-products of Cybium Niphonium Using Subcritical Fluid Extraction Method[J].Journal of Ningbo University(Natural Science & Engineering Edition),2012,25(04):10-15.DOI:
| Title: | Fish Oil Extraction from By-products of Cybium Niphonium Using Subcritical Fluid Extraction Method |
| 作者: | 毛丽芳, 朱新亮, 桑卫国 |
| Author(s): | MAO Li-fang, ZHU Xin-liang, SANG Wei-guo |
| 关键词: | 亚临界流体萃取; 二甲醚; 马鲛鱼; 鱼油 |
| Keywords: | sub-critical extraction; dimethyl ether; scombermorus; fish oil |
| 分类号: | S985.1+3 |
| 文献标识码: | A |
| 摘要: | 以二甲醚为萃取溶剂, 萃取压力始终控制在0.8~1.0MPa, 优选亚临界流体萃取马鲛鱼加工下脚料中鱼油工艺条件. 以马鲛鱼油萃取得率为考查指标, 对影响鱼油提取工艺的因素进行了研究. 通过单因素试验探讨了萃取时间、萃取温度、萃取次数对萃取效果的影响, 利用L4(23)正交试验法优化亚临界流体萃取马鲛鱼加工下脚料中鱼油的最佳工艺条件. 试验结果表明: 亚临界流体萃取马鲛鱼油的最佳条件为萃取时间45min, 萃取温度40℃, 萃取3次, 在此条件下马鲛鱼油萃取得率为73.52%, 所得马鲛鱼油各项指标均达到一级油标准. 揭示亚临界流体萃取技术应用于鱼油生产, 具有成本低, 经济效益好的良好前景. |
| Abstract: | In this study, the efficacy of subcritical extraction techniques is investigated for extracting fish oil from by-products of Cybium Niphonium. In our experiment, dimethyl ether (DME) was used as an extracting medium, the extracting pressure was set up at 0.8-1.0MPa. Taking the extraction yield of Cybium Niphonium oil as the examination target, the factors influencing fish oil extraction were observed and recorded. First, discussions are made on the extract time, the extract temperature, and the extract times, all of which are based on the single factor experiment to withdraw the effect the influence. Then an orthogonal experimental design was used, in which the fish oil yield is used as a dependent variable, and the independent variables include extracting time, extracting temperature and extracting times. The results show that the optimal extracting conditions for maximum oil yield are as follows: 45min extracting time, 40℃ extracting temperature, and 3 extracting times, which generates the oil yield of 73.52%. This study suggests that application of subcritical extraction technology in extraction of fish oil from Cybium Niphonium is an effective and economic approach for producing high quality fish oil at low cost. |
| 参考文献 /References: | [1] 刘平怀, 时杰, 沈世军. 亚临界萃取法回收废弃虾蟹壳中虾青素[J]. 精细化工, 2011, 28(5):497-500. [2] Mustapa A, Manan Z, Mohd Azizi C, et al. Extraction of β-carotenes from palm oil mesocarp using sub-critical R134a[J]. Food Chemistry, 2011, 125:262-267. [3] 林承杰, 张力, 刘明金, 等. 玫瑰精油真空水散冲蒸亚临界流体萃取技术: 中国, 101096614[P]. 2008-01-02. [4] 李超, 郑义, 王卫东, 等. 响应曲面法优化亚临界水提取葡萄籽原花青素的工艺研究[J]. 食品科学, 2010, 31(12):6-10. [5] 刘玉梅, 刘奎钫, 石波, 等. 一种生产番茄红素油树脂的方法: 中国, 101928473[P]. 2010-12-29. [6] 何蓉蓉, 张延延, 曹云峰, 等. 五味子提取物及其制备方法和应用: 中国, 101978990[P]. 2011-02-23. [7] 林长华. 漫话马鲛鱼[J]. 中国水产, 2011(3):78-79. [8] 黄克勤. 马鲛鱼[J]. 水产科技情报, 1973(11):31. [9] 娄永江, 杨文鸽, 王扬, 等. 马鲛鱼方便食品的开发[J]. 食品科技, 2000(6):31. [10] 李西腾. 马鲛鱼丸的加工工艺研究[J]. 农业科技与装备, 2011(7):26-29. |
| 备注/Memo: | 收稿日期: 2012-05-20. 基金项目: 浙江省科技厅科研项目(2010R50029). 第一作者: 毛丽芳(1988-), 女, 福建泉州人, 在读硕士研究生, 主要研究方向: 水产品综合利用. E-mail: maolifang2010@163.com *通讯作者: 桑卫国(1955-), 男, 浙江宁波人, 副教授, 主要研究方向: 功能性食品油脂研究. E-mail: sangweiguo@nbu.edu.cn 宁波大学学报(理工版)网址:http://journallg.nbu.edu.cn/ |